Vol. 51
Latest Volume
All Volumes
PIERB 105 [2024] PIERB 104 [2024] PIERB 103 [2023] PIERB 102 [2023] PIERB 101 [2023] PIERB 100 [2023] PIERB 99 [2023] PIERB 98 [2023] PIERB 97 [2022] PIERB 96 [2022] PIERB 95 [2022] PIERB 94 [2021] PIERB 93 [2021] PIERB 92 [2021] PIERB 91 [2021] PIERB 90 [2021] PIERB 89 [2020] PIERB 88 [2020] PIERB 87 [2020] PIERB 86 [2020] PIERB 85 [2019] PIERB 84 [2019] PIERB 83 [2019] PIERB 82 [2018] PIERB 81 [2018] PIERB 80 [2018] PIERB 79 [2017] PIERB 78 [2017] PIERB 77 [2017] PIERB 76 [2017] PIERB 75 [2017] PIERB 74 [2017] PIERB 73 [2017] PIERB 72 [2017] PIERB 71 [2016] PIERB 70 [2016] PIERB 69 [2016] PIERB 68 [2016] PIERB 67 [2016] PIERB 66 [2016] PIERB 65 [2016] PIERB 64 [2015] PIERB 63 [2015] PIERB 62 [2015] PIERB 61 [2014] PIERB 60 [2014] PIERB 59 [2014] PIERB 58 [2014] PIERB 57 [2014] PIERB 56 [2013] PIERB 55 [2013] PIERB 54 [2013] PIERB 53 [2013] PIERB 52 [2013] PIERB 51 [2013] PIERB 50 [2013] PIERB 49 [2013] PIERB 48 [2013] PIERB 47 [2013] PIERB 46 [2013] PIERB 45 [2012] PIERB 44 [2012] PIERB 43 [2012] PIERB 42 [2012] PIERB 41 [2012] PIERB 40 [2012] PIERB 39 [2012] PIERB 38 [2012] PIERB 37 [2012] PIERB 36 [2012] PIERB 35 [2011] PIERB 34 [2011] PIERB 33 [2011] PIERB 32 [2011] PIERB 31 [2011] PIERB 30 [2011] PIERB 29 [2011] PIERB 28 [2011] PIERB 27 [2011] PIERB 26 [2010] PIERB 25 [2010] PIERB 24 [2010] PIERB 23 [2010] PIERB 22 [2010] PIERB 21 [2010] PIERB 20 [2010] PIERB 19 [2010] PIERB 18 [2009] PIERB 17 [2009] PIERB 16 [2009] PIERB 15 [2009] PIERB 14 [2009] PIERB 13 [2009] PIERB 12 [2009] PIERB 11 [2009] PIERB 10 [2008] PIERB 9 [2008] PIERB 8 [2008] PIERB 7 [2008] PIERB 6 [2008] PIERB 5 [2008] PIERB 4 [2008] PIERB 3 [2008] PIERB 2 [2008] PIERB 1 [2008]
2013-05-06
A Free-Space Method for Complex Permittivity Measurement of Bulk and Thin Film Dielectrics at Microwave Frequencies
By
Progress In Electromagnetics Research B, Vol. 51, 307-328, 2013
Abstract
A free-space, non-destructive method for measuring the complex permittivity of a double-layer bulk dielectrics and thin film oxide layers at microwave frequencies have been developed. The method utilizes a spot-focusing antenna system in conjunction with a vector network analyzer in the range of 18-26 GHz. The bulk dielectric was measured using the Transmission Method and Metal-Backed Method, while the Metal-Backed Method was used to investigate the thin films. Both types of samples were sandwiched between two quarter-wavelength Teflon plates to improve the mismatch at the frequencies of measurement. The thin film sample arrangement was backed by an additional metal plate. The double-layer bulk dielectric samples were Teflon-PVC and Plexiglas-PVC, while the thin film samples consisted of SiO2 layers of different thicknesses grown on doped and undoped Si wafer substrates. The relative permittivity obtained for PVC ranged between 2.62 to 2.93, while those for Plexiglas exhibited values between 2.45 to 2.63. The relative permittivity of SiO2 deposited on these wafers was between 3.5 to 4.5. All these values were in good agreement with published data The advantage of the method was its ability to measure the dielectric properties of the films at the mid-frequency band irrespective of the substrate type used. Simulations of the measurement setup were carried out using CST Microwave Studio and the simulation results agreed closely with the measurements.
Citation
Zaiki Awang, Fatimah Audah Mohd Zaki, Noor Hasimah Baba, Ahmad Sabirin Zoolfakar, and Raudah Abu Bakar, "A Free-Space Method for Complex Permittivity Measurement of Bulk and Thin Film Dielectrics at Microwave Frequencies," Progress In Electromagnetics Research B, Vol. 51, 307-328, 2013.
doi:10.2528/PIERB13031509
References

1. Hambley, A. R., Electronics, 2nd Ed., Prentice-Hall International, Inc., New Jersey, 2000.

2. Ahmad, S., Microwave and Millimeter Wave Semiconductor Materials Technology, Tata McGraw-Hill, New York, 1998.

3. Baba, N. H., Z. Awang, and D. K. Ghodgaonkar, "Accuracy considerations for dielectric measurements of semiconductor wafers using free space microwave measurement system in 8-13 GHz range," Proc. IEEE Int. RF and Microwave Conf. (RFM), 177-181, Kuala Lumpur, Oct. 5-6, 2004.

4. Saad, T. S., R. C. Hansen, and G. J. Wheeler, Microwave Engineers' Handbook, Vol. 1, 179, Artech House, Boston, 1971.

5. Ghodgaonkar, D. K., V. V. Varadan, and V. K. Varadan, "Free-space measurement of complex permittivity and complex permeability of magnetic materials at microwave frequencies," IEEE Trans. of Inst. and Measurement, Vol. 39, No. 2, 387-394, Apr. 1990.
doi:10.1109/19.52520

6. Srivastava, G. P. and V. L. Gupta, Microwave Devices and Circuit Design, Prentice-Hall India, New Delhi, 2006.

7. Ghodgaonkar, D. K., V. V. Varadan, and V. K. Varadan, "A free-space method for measurement of dielectric constants and loss tangents at microwave frequencies," IEEE Trans. of Inst. and Measurement, Vol. 38, No. 3, 789-793, Jun. 1989.
doi:10.1109/19.32194

8. Baba, N. H., Microwave Non-destructive Testing of Semiconductor Materials, M.Sc. thesis, Universiti Teknologi MARA, Apr. 2005.

9. Millitech, Inc., Series GOA Gaussian Optics Lens Antenna.

10. Hippel, A. V., Dielectric Materials and Applications, Artech House, Boston, 1995.

11. Zant, P. V., Microchip Fabrication, 5th Ed., McGraw-Hill, New York, 2004.

12. Kasap, S. O., Principles of Electronic Materials and Devices, 2nd Ed., McGraw-Hill, New York, 2002.

13. Kawate, E. and B. Prijamboedi, "Development of the measurement method of dielectric constant of low-k film in the millimeter wave region," Proc. Joint 29th Int. Conf. on Infrared and Millimeter Waves and 12th Int. Conf. on Terahertz Electronics, 801-802, Karlsruhe, Germany, Oct. 2004.

14. Bakker, G. L. and D. W. Hess, "Removal of thermally grown SiO2 films using water at elevated temperature and pressure," Electrochem. Soc. Proc., Vol. 95-20, 464-471, 1996.

15. Harper, C. A., Handbook of Ceramics, Glasses and Diamonds, McGraw-Hill, New York, 2001.

16. Baker-Jarvis, J., et al. "Dielectric characterization of low-loss materials: A comparison technique," IEEE Trans. Dielectric Elect. Ins., Vol. 5, No. 4, 571-577, Aug. 1998.
doi:10.1109/94.708274

17. Albertin, K. F., M. A. Valle, and I. Pereyra, "Study of MOS capacitors with TiO2 and SiO2/TiO2 gate dielectric," J. Int. Cir. Systems, Vol. 2, 89-93, 2007.

18. Shackelford, J. F., W. Alexander, and J. S. Park, Materials Science and Engineering, 2nd Ed., CRC Press, Inc., Boca Raton, 1994.

19. May, G. S. and S. M. Sze, Fundamentals of Semiconductor Fabrication, John Wiley and Sons, New York, 2004.

20. Schroder, D. K., Semiconductor Material and Device Characterization, 2nd Ed., John Wiley & Sons, Inc., New York, 2004.

21. Hadi, D. A., S. F. W. M. Hatta, and N. Soin, "Effect of oxide thickness on 32nm PMOSFET reliability," Proc. IEEE Int. Conf. on Semicond. Electron. (ICSE), 244-247, Jun. 28-30, 2010.

22. Mahapatra, S., M. A. Alam, P. B. Kumar, T. R. Dalei, D. Varghese, and D. Saha, "Negative bias temperature instability in CMOS devices," Microelectronics Eng., Vol. 80, 114-121, 2005.
doi:10.1016/j.mee.2005.04.053

23. Alam, M. A., H. Ku°uoglu, D. Varghese, and S. Mahapatra, "A comprehensive model for PMOS NBTI degradation: Recent progress," Microelectronics Rel., Vol. 47, 853-862, Dec. 2006.

24. Kwan, W. S. and M. J. Deen, "Hot-carrier effects on the scattering parameters of lightly doped drain n-type metal-oxide-semiconductor field effect transistor ," J. Vac. Sci. Technol., Vol. 16, No. 2, 628-632, Jan. 1998.

25. Nevin, W. A. and G. A. Chamberlain, "Effect of oxide thickness on the properties of metal-insulator-organic semiconductor photovoltaic cells," IEEE Trans. on Electron. Devices, Vol. 40, No. 1, 75-81, Jan. 1993.
doi:10.1109/16.249427

26. Burkhardt, P. J., "Dielectric relaxation in thermally grown SiO2 films," IEEE Trans. on Elect. Dev., Vol. 13, No. 2, 268-275, Feb. 1966.
doi:10.1109/T-ED.1966.15679

27. Ismail, M. Y., M. Inam, and A. M. A. Zaidi, "Reflectivity of reflectarrays based on dielectric substrates," Amer. J. of Eng. Appl. Sci., Vol. 3, No. 1, 180-185, 2010.
doi:10.3844/ajeassp.2010.180.185

28. Wheeler, H. A., "Formulas for the skin effect," Proc. of the IRE, Vol. 30, No. 9, 412-424, Sept. 1942.

29. Bichara, M. R. E. and J. P. R. Poitevin, "Resistivity measurement of semiconducting epitaxial layers by the reflection of a hyperfrequency electromagnetic wave," IEEE Trans. Inst. Meas., Vol. 13, 323-328, Dec. 1964.
doi:10.1109/TIM.1964.4313421